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• W4237119794 abstract "Angewandte Chemie International Edition in EnglishVolume 22, Issue 12 p. 990-991 Communication Tricyclo[2.1.0.02,5]pentan-3-one†‡ Prof. Dr. Günther Maier, Corresponding Author Prof. Dr. Günther Maier Institut für Organische Chemie der Universität, Heinrich-Buff-Ring 58, D-6300 Giessen (Germany)Institut für Organische Chemie der Universität, Heinrich-Buff-Ring 58, D-6300 Giessen (Germany)Search for more papers by this authorManfred Hoppe, Manfred Hoppe Institut für Organische Chemie der Universität, Heinrich-Buff-Ring 58, D-6300 Giessen (Germany)Search for more papers by this authorDr. Hans Peter Reisenauer, Dr. Hans Peter Reisenauer Institut für Organische Chemie der Universität, Heinrich-Buff-Ring 58, D-6300 Giessen (Germany)Search for more papers by this author Prof. Dr. Günther Maier, Corresponding Author Prof. Dr. Günther Maier Institut für Organische Chemie der Universität, Heinrich-Buff-Ring 58, D-6300 Giessen (Germany)Institut für Organische Chemie der Universität, Heinrich-Buff-Ring 58, D-6300 Giessen (Germany)Search for more papers by this authorManfred Hoppe, Manfred Hoppe Institut für Organische Chemie der Universität, Heinrich-Buff-Ring 58, D-6300 Giessen (Germany)Search for more papers by this authorDr. Hans Peter Reisenauer, Dr. Hans Peter Reisenauer Institut für Organische Chemie der Universität, Heinrich-Buff-Ring 58, D-6300 Giessen (Germany)Search for more papers by this author First published: December 1983 https://doi.org/10.1002/anie.198309901Citations: 22 † Small Rings. Part 49. This work was supported by the Deutsche Forschungsgemeinschaft.—Part 48: T. Loerzer, R. Machinek, W. Lüttke, L. H. Franz, K.-D. Malsch, G. Maier, Angew. Chem. 95 (1983) 914; Angew. Chem. Int. Ed. Engl. 22 (1983) 878. ‡ Dedicated to Professor Karl Winacker on the occasion of his 80th birthday AboutPDF ToolsRequest permissionExport citationAdd to favoritesTrack citation ShareShare Give accessShare full text accessShare full-text accessPlease review our Terms and Conditions of Use and check box below to share full-text version of article.I have read and accept the Wiley Online Library Terms and Conditions of UseShareable LinkUse the link below to share a full-text version of this article with your friends and colleagues. Learn more.Copy URL No abstract is available for this article. References 1(a) W.-D. Stohrer, R. Hoffmann, J. Am. Chem. Soc. 94 (1972) 1661; (b) A. Schweig, W. Thiel, Tetrahedron Lett. 1978, 1841; J. Comput. Chem. 1 (1980) 129; K. B. Lipkowitz, J. Am. Chem. Soc. 100 (1978) 7535. 2 G. Maier, S. Pfriem, U. Schäfer, K.-D. Malsch, R. Matusch, Chem. Ber. 114 (1981) 3965. 3(a) G. Maier, M. Hoppe, H. P. Reisenauer, C. Krüger, Angew. Chem. 94 (1982) 445; Angew. Chem. Int. Ed. Engl. 21 (1982) 437; Angew. Chem. Suppl. 1982, 1061; (b) H. W. Lage, H. P. Reisenauer, G. Maier, Tetrahedron Lett. 23 (1982) 3893; (c) G. Maier, U. Schäfer, W. Sauer, H. Hartan, J. F. M. Oth, Tetrahedron Lett. 1978, 1837. 4(a) M. Christl, Chem. Ber. 108 (1975) 2781; (b) M. Christl, H.-J. Lüddeke, A. Nagyrevi-Neppel, G. Freitag, Chem. Ber. 110 (1977) 3745; (c) M. Christl, R. Herbert, Chem. Ber. 112 (1979) 2022; (d) in tricyclo[2.1.0.02,5]pentane [G. D. Andrews, J. E. Baldwin, J. Am. Chem. Soc. 99 (1977) 4851] the 13CH coupling constant of C-1/C-3 of 210 Hz certainly corresponds to the expectation value but not the chemical shift of this C-atom (δ = 20.8), which in comparison to 3 and the numerous bicyclobutane derivatives investigated by Christl appears at extremely low field. 5 A weak band at 927 cm−1 cannot be assigned to any of the products mentioned. It is curious that tetrahedrane 4 should exhibit its only intense IR absorption in this region (940 cm−1): J. M. Schulman, J. Venanzi, J. Am. Chem. Soc. 96 (1974) 4739. Citing Literature Volume22, Issue12December 1983Pages 990-991 ReferencesRelatedInformation" @default.
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