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- W4237512008 abstract "The C19–C30 bis-THF fragment of the proposed structure of iriomoteolide-13a has been synthesized. The w-mesyloxy-substituted stereotetrad possessing three continuous hydroxy groups was generated by <i>anti</i>-aldol reaction and asymmetric dihydroxylation (AD). Upon heating in pyridine the stereotetrad underwent an S<sub>N</sub>2 cyclization to form the C19–C22 THF ring. It was followed by an intramolecular <i>syn</i>-oxypalladation of the C28 chiral allylic alcohol to give the C23–C26 THF ring." @default.
- W4237512008 created "2022-05-12" @default.
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- W4237512008 date "2020-12-31" @default.
- W4237512008 modified "2023-10-16" @default.
- W4237512008 title "Synthesis of the C19–C30 Bis-THF Fragment of Iriomoteolide-13a via Stepwise SN2 Cyclization and Intramolecular syn-Oxypalladation" @default.
- W4237512008 doi "https://doi.org/10.26434/chemrxiv.13506678" @default.
- W4237512008 hasPublicationYear "2020" @default.
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