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- W4238172020 endingPage "16421" @default.
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- W4238172020 abstract "Abstract Cycloadditions are powerful processes to synthesize complex polycyclic scaffolds. Herein, we disclose a [4+3]‐cycloaddition between an in situ generated ortho ‐quinone methide and an isomünchnone to yield oxa‐bridged oxazocine cores, generating N 2 and H 2 O as the sole by‐products. Using only catalytic amounts of camphorsulfonic acid, it is possible to generate both reactive intermediates in one step, eliminating the need for rhodium catalysts generally employed for isomünchnone formation. Spectroscopic data and X‐ray crystallography indicate the formation of the syn diastereomer, with the main side‐product arising from a hydrate participating in a competing [4+2]‐cycloaddition pathway." @default.
- W4238172020 created "2022-05-12" @default.
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- W4238172020 date "2018-11-11" @default.
- W4238172020 modified "2023-10-17" @default.
- W4238172020 title "Transition‐Metal‐Free [4+3]‐Cycloaddition of <i>ortho</i>‐Quinone Methides and Isomünchnones: Catalytic and Diastereoselective Assembly of Oxa‐bridged Oxazocine Scaffolds" @default.
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- W4238172020 doi "https://doi.org/10.1002/ange.201810760" @default.
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