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- W4238575687 abstract "EPR in single crystals of NiTiF6⋅6H2O has been studied in the frequency ranges 12–18 GHz and 23–25 GHz. A phase transition from the room temperature trigonal structure to a lower symmetry structure takes place at a temperature between 134 and 137 °K for a slowly cooled sample. The reverse transition occurs at approximately 141 °K. As the phase transition takes of the order of 10 min for completion, the trigonal phase may be retained at low temperatures by rapidly cooling the sample below about 100 °K. In the trigonal phase above 4.2 °K, both g∥ and g⊥ are approximately 2.27 and the crystal field parameter D has the magnitude (1.30±0.01) cm−1 at 4.2 °K, (1.337±0.005) cm−1 at 77 °K, and (1.31±0.01) cm−1 at 298 °K. The data for the trigonal phase below 4.2 °K may be represented by divergent g values, with g∥?2.50 and g⊥?2.20 at 1.3 °K. In the low symmetry phase, with g∥ assumed to be 2.25, the crystal field parameters at 77 °K are ‖D‖?2.0 cm−1 and ‖E‖?0.20 cm−1." @default.
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- W4238575687 date "1976-04-15" @default.
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- W4238575687 title "Electron paramagnetic resonance in nickel fluotitanate" @default.
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- W4238575687 doi "https://doi.org/10.1063/1.432624" @default.
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