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- W4240932125 abstract "Abstract Chiral tertiary diaryl carbinols are key intermediates for the synthesis of pharmacologically active compounds. This article describes the procedure for the catalytic enantioselective addition of an in‐situ prepared aryltitanium reagent to p‐chloroacetophenone: (R)‐(+)‐1‐(4‐chlorophenyl)‐1‐m‐tolylethanol. It presents some of the important points to be considered, the conditions that need to be maintained, characterization data, and the reagents required, as well as the techniques used and the equipment setup that are vital to carrying out the process. For the enantioselective synthesis, much effort has been directed toward the development of the catalytic enantioselective arylation of alkyl aryl ketones. Catalytic methods utilizing arylzinc, ‐aluminum, ‐titanium, and ‐boron reagents are explored. However, reactions are generally carried out at relatively large catalyst loadings, making them less practical for scale‐up applications. The article also describes the hazards associated with working with chemicals and the ways to deal with these hazards." @default.
- W4240932125 created "2022-05-12" @default.
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- W4240932125 date "2020-04-29" @default.
- W4240932125 modified "2023-10-14" @default.
- W4240932125 title "Catalytic Enantioselective Addition of an In‐Situ Prepared Aryltitanium Reagent to <i>p</i> ‐Chloroacetophenone: ( <i>R</i> )‐(+)‐1‐(4‐Chlorophenyl)‐1‐ <i>m</i> ‐Tolylethanol" @default.
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- W4240932125 doi "https://doi.org/10.1002/0471264229.os096.21" @default.
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