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• W4241636106 abstract "Abstract The introduction of high‐frequency, high‐power microwave sources, tailored biradicals, and low‐temperature magic angle spinning (MAS) probes has led to a rapid development of hyperpolarization strategies for solids and frozen solutions, leading to large gains in NMR sensitivity. Here, we introduce a protocol for efficient hyperpolarization of 19 F nuclei in MAS DNP enhanced NMR spectroscopy. We identified trifluoroethanol‐ d 3 as a versatile glassy matrix and show that 12 m m AMUPol (with microcrystalline KBr) provides direct 19 F DNP enhancements of over 100 at 9.4 T. We applied this protocol to obtain DNP‐enhanced 19 F and 19 F– 13 C cross‐polarization (CP) spectra for an active pharmaceutical ingredient and a fluorinated mesostructured hybrid material, using incipient wetness impregnation, with enhancements of approximately 25 and 10 in the bulk solid, respectively. This strategy is a general and straightforward method for obtaining enhanced 19 F MAS spectra from fluorinated materials." @default.
• W4241636106 created "2022-05-12" @default.
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• W4241636106 date "2019-04-23" @default.
• W4241636106 modified "2023-09-30" @default.
• W4241636106 title "¹⁹ F Magic Angle Spinning Dynamic Nuclear Polarization Enhanced NMR Spectroscopy" @default.
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• W4241636106 doi "https://doi.org/10.1002/ange.201814416" @default.
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