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- W4242822010 abstract "The electrochemical polymerization of N-trimethylsilylethoxymethyl-3-methyl-4-pyrrole carboxylate ethyl ester (MPCE-SEM) in the presence of pyrrole, to give free-standing copolymer films is described. These films have been characterized by surface conductivity measurements, reflectance FTIR spectroscopy, X-ray photoelectron spectroscopy and scanning electron microscopy. Increasing the relative concentration of MPCE-SEM in the polymerization solution resulted in an increase in the proportion of these units in the copolymer film. Increasing the proportion of MPCE-SEM units in the copolymer resulted in a decrease in surface conductivity. This is consistent with expectation because N-substituted polypyrroles tend to have lower conductivity values than unsubstituted polypyrrole. Significantly, it has also been shown that the N-protecting group of the MPCE-SEM unit can be removed after polymerization under mild conditions in a solid phase deprotection procedure. © 1998 Society of Chemical Industry" @default.
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- W4242822010 date "1998-09-01" @default.
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- W4242822010 title "Structure and conductivity in substituted polypyrroles. Part 1. Synthesis and electropolymerization of N-trimethylsilylethoxymethyl-3-methyl-4-pyrrole carboxylate ethyl ester" @default.
- W4242822010 doi "https://doi.org/10.1002/(sici)1097-0126(199809)47:1<43::aid-pi46>3.3.co;2-b" @default.
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