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• W4243039594 abstract "[1078-58-6] C12H10Zn (MW 219.59) InChI = 1S/2C6H5.Zn/c2*1-2-4-6-5-3-1;/h2*1-5H; InChIKey = MKRVHLWAVKJBFN-UHFFFAOYSA-N (used in a Michael 1,4-addition or as a reactive coupling partner in Negishi cross-coupling) Alternative Name: zinc diphenyl. Physical Data: bp 180 °C at 6.58 × 102 Pa,1 mp 105–106 °C,2 white solid, air and moisture sensitive, hazardous. Solubility: soluble in most organic solvents. Form Supplied in: >92% pure (Aldrich), <7.5% benzene, in glass bottle, solid; or 99% (Strem Chemicals). Analysis of Reagent Purity:3 1H NMR (THF-d8, 250 MHz): δ 7.61 (dd, J = 7, 4 Hz, 4H (aryl-H, 2,6-H)), 7.15 (dd, J = 7 Hz, 4H (aryl-H, 3,5-H)), 7.08 (t, J = 7 Hz, 2H (aryl-H, 4-H)). Handling, Storage, and Precautions: inhalation of the zinc oxide fumes produced from this compound in a fire may cause ‘metal fume fever' or ‘zinc shakes' consisting of chills, fever, muscular pain, nausea, and vomiting. Irritating to skin, eyes, and respiratory tract. Inhalation may cause chills and nausea. Use in a laboratory fume hood with safe glasses, a laboratory coat, and safety gloves. Preparative Method: the reagent is prepared via reaction of zinc chloride with PhMgBr or from elemental zinc and diphenylmercury." @default.
• W4243039594 created "2022-05-12" @default.
• W4243039594 creator A5051016251 @default.
• W4243039594 date "2013-04-22" @default.
• W4243039594 modified "2023-10-16" @default.
• W4243039594 title "Diphenylzinc" @default.
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• W4243039594 doi "https://doi.org/10.1002/047084289x.rn01548" @default.
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