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- W4243837439 abstract "Abstract A 1,3‐diphosphacyclobutane‐2,4‐diyl contains a unique unsaturated cyclic unit, and the presence of radical‐type centers have been expected as a source of functionality. This study demonstrates that the P‐heterocyclic singlet biradical captures muonium (Mu=[μ + e − ]), the light isotope of a hydrogen radical, to generate an observable P‐heterocyclic paramagnetic species. Investigation of a powder sample of 2,4‐bis(2,4,6‐tri‐ t ‐butylphenyl)‐1‐ t ‐butyl‐3‐benzyl‐1,3‐diphosphacyclobutane‐2,4‐diyl using muon (avoided) level‐crossing resonance (μLCR) spectroscopy revealed that muonium adds to the cyclic P 2 C 2 unit. The muon hyperfine coupling constant ( A μ ) indicated that the phosphorus atom bearing the t ‐butyl group trapped muonium to provide a metastable P‐heterocyclic radical involving the ylidic MuP(<)=C moiety. The observed regioselective muonium addition correlates the canonical formula of 1,3‐diphosphacyclobutane‐2,4‐diyl." @default.
- W4243837439 created "2022-05-12" @default.
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- W4243837439 date "2018-06-14" @default.
- W4243837439 modified "2023-10-16" @default.
- W4243837439 title "Observation of a Metastable P‐Heterocyclic Radical by Muonium Addition to a 1,3‐Diphosphacyclobutane‐2,4‐diyl" @default.
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- W4243837439 doi "https://doi.org/10.1002/ange.201804306" @default.
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