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- W4244021666 abstract "One of the first applications of palladium to indole synthesis was due to Hegedus, who adapted the known palladium (Pd)-mediated amination of alkenes to the intramoleclar amination of o-vinyl or o-allylanilines. Although it is rarely referred to as such, the Hegedus reaction has found several applications and extensions in indole synthesis. The preparation of ethyl indole-2-carboxylates has been improved by McNulty and Keskar, and Danheiser synthesized 6-n-butyl-1,2-dimethyl-4-hydroxyindole via a benzannulation of a cyclobutenone and an ynamide, and subsequent Pd-catalyzed cyclization. The synthesis of both paspalinine and (±)-lecanindole-D featured a Hegedus indolization. Li, Deng, and coworkers employed allylic esters with o-iodoanilines and PdCl2 (n-Bu4NCl, K2CO3, DMA, 100 degrees C) to give indoles in yields up to 88%. Ghorai and colleagues adapted the Hegedus protocol to access a series of 3-substituted 2-benzylindoles." @default.
- W4244021666 created "2022-05-12" @default.
- W4244021666 date "2016-06-17" @default.
- W4244021666 modified "2023-09-23" @default.
- W4244021666 title "Palladium-Catalyzed Indole Ring Synthesis" @default.
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- W4244021666 doi "https://doi.org/10.1002/9781118695692.ch70" @default.
- W4244021666 hasPublicationYear "2016" @default.
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