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- W4244128907 abstract "An efficient synthesis of 3-hydroxyisoxazoles from β-ketoesters and hydroxylamine was investigated. The reaction of the sodium salts of β-ketoesters and hydroxylamine at a low temperature, followed by quenching with an excess of cone. HC1 under heating gave predominantly 3-hydroxyisoxazoles involving 4-sulfenylated 3-hydroxyisoxazoles. Starting from the prepared 4-(2, 4-dichlorobenzyl)-3-hydroxy-5-methylisoxazole, a potential herbicidal compound, 4-(2, 4-dichlorobenzoyl)-3-hydroxy-5-methylisoxazole, was also synthesized in five steps." @default.
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- W4244128907 date "1986-01-01" @default.
- W4244128907 modified "2023-09-26" @default.
- W4244128907 title "Synthesis of 3-hydroxyisoxazoles from .BETA.-ketoesters and hydroxylamine." @default.
- W4244128907 doi "https://doi.org/10.1271/bbb1961.50.1831" @default.
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