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- W4244967189 abstract "Synthesis and polymerization of novel 2-trifluoromethyl-3-(2-tetrahydrofuranyl)-1-propyl 2-trifluoromethylacrylate [CH2=C(CF3)COOCH2CH(CF3)CH2(C4H7O)] were developed. The fluorinated ester alkyl moiety was synthesized by reduction of the compound from the radical addition of tert-butyl 2-trifluoromethylacrylate [CH2=C(CF3)COOC4H9] with tetrahydrofuran. The fluoroalkyl 2-trifluoromethylacrylate was synthesized by the reaction of 2-trifluoromethylacryloyl chloride with the fluorinated alcohol. Radical and anionic polymerizations of the monomer were examined to afford a polymer of 1.0 × 104 as the highest molecular weight initiated by 2,2′-azobisisobutyronitrile at 60 °C in spite of the low yield of the polymer, though ethyl 2-trifluoromethylacrylate showed poor polymerization reactivity under radical conditions." @default.
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- W4244967189 date "2011-09-14" @default.
- W4244967189 modified "2023-09-26" @default.
- W4244967189 title "Synthesis and polymerization of novel fluoroalkyl 2-trifluoromethylacrylate possessing tetrahydrofuran moiety" @default.
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- W4244967189 doi "https://doi.org/10.1002/pola.24955" @default.
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