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- W4245570108 abstract "An electrochemical synthesis of 5,6,7,8-tetrahydrofolic acid (H4PteGlu) from folic acid (PteGlu) has been developed. In the first step folic acid is reduced, via 5,8-dihydrofolic acid (5,8-H2PteGlu), to 7,8-H2PteGlu. Reduction of the protonated 7,8-H2PteGlu cleaves C(9)-N(10), but reduction of the unprotonated compound at a more negative potential leads to H4PteGlu in high yield. The reduction is made at relatively low buffer concentration which permits having a neutral pH in the bulk of the solution, but a high pH at the electrode surface due to the electrogenerated base. Besides the preparation of H4PteGlu, the reduction of 5,10-methylidyne-H4PteGlu and 5,10-methylene-H4PteGlu was studied." @default.
- W4245570108 created "2022-05-12" @default.
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- W4245570108 date "1979-09-01" @default.
- W4245570108 modified "2023-09-25" @default.
- W4245570108 title "295 - Preparation of tetrahydrofolic acid and related compounds by electrochemical methods" @default.
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- W4245570108 doi "https://doi.org/10.1016/0302-4598(79)80010-0" @default.
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