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- W4245647532 abstract "Gut ausgebildete Kristalle (würfel- bzw. quaderförmig; Kantenlänge bis ca. 1 mm) von rhomboedrischem Cr2(SO4)3 wurden mit Cl2 oder HCl als Transportmittel (z. B. 690 → 630°C) auf der weniger heißen Seite einer Quarzglasampulle abgeschieden. Mit beiden Transportmitteln können hohe Transportleistungen (z. B. 78 mg/h) erzielt werden. Es wurde der Einfluß der Temperatur sowie der Transportmittelkonzentration (Zusatz von PtCl2) auf die Abscheidungsraten untersucht. Auf der Basis thermodynamischer Modellrechnungen wird eine Interpretation des beobachteten, auf endotherme Reaktionen zurückzuführenden Transportverhaltens gegeben. Contributions on the Thermal Behaviour of Sulfates. XIII. The Chemical Vapour Transport of Cr2(SO4)3 with Cl2 and with HCl. Experiments and Calculations Well shaped crystals (cubical or rectangular parallel-epiped respectively, edge length up to 1 mm) of rhombohedral Cr2(SO4)3 can be grown in the less hot zone of a closed silica ampoule by means of CVT using Cl2 or HCl as transport agents in endothermal transport reactions. The influence of the mean transport temperature as well as the concentration of the transport agents on the deposition rates was investigated. On the basis of thermochemical calculations an explanation of the transport mechanism is given in the present paper." @default.
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- W4245647532 date "1994-09-01" @default.
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- W4245647532 title "Beitr�ge zum thermischen Verhalten von Sulfaten. XIII. Zum chemischen Transport von Cr2(SO4)3 mit Cl2 und mit HCl. Experimente und Modellrechnungen" @default.
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- W4245647532 doi "https://doi.org/10.1002/zaac.19946200913" @default.
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