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- W4246156738 abstract "Sterically shielded nitroxides of pyrrolidine series are known to demonstrate the highest stability to reduction. Here we report on the synthesis of new pyrrolidine nitroxides from 5,5-dialkyl-1-pyrroline N -oxides via the introduction of pent-4-enyl group to nitrone atom followed by intramolecular 1,3-dipolar cycloaddition reaction and isoxazolidine ring opening. Kinetics of reduction of the new nitroxides with ascorbate was studied and compared to that of previously published 1 S ,2 R ,3′ S ,4′ S ,5′ S ,2″ R -dispiro[(2-hydroxymethyl)-cyclopentan-1,2′-(3′,4′-di- tert -butoxy)pyrrolidine-5′,1″-(2″-hydroxymethyl)cyclopentane]-1′-oxyl ( 1 )." @default.
- W4246156738 created "2022-05-12" @default.
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- W4246156738 date "2019-06-03" @default.
- W4246156738 modified "2023-09-24" @default.
- W4246156738 title "Synthesis of 1-azaspiro[4.4]nonan-1-oxyls via Intramolecular 1,3-Dipolar Cycloaddition" @default.
- W4246156738 doi "https://doi.org/10.3762/bxiv.2019.37.v1" @default.
- W4246156738 hasPublicationYear "2019" @default.
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