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- W4246629945 abstract "[2471-91-2] C8H8O2S (MW 168.21) (a source of o-quinodimethanes1 that are useful diene intermediates in Diels–Alder reactions; a source of benzocyclobutene) Physical Data: mp 150–151 °C. Solubility: sol EtOH, CHCl3, C6H6, boiling water; slightly sol Et2O. Preparative Methods: by oxidation of 1,3-dihydrobenzo[c]thiophene;2 from α,α′‐Dibromo‐o‐xylene, rongalite (Sodium Hydroxymethanesulfinate, HOCH2SO2Na·2H2O), and Sulfur Dioxide.3 Purification: recrystallization (H2O; H2O–EtOH; CH2Cl2–petroleum ether; CHCl3–C6H6; C6H6–petroleum ether). Handling, Storage, and Precautions: unstable to alkali and concentrated H2SO4." @default.
- W4246629945 created "2022-05-12" @default.
- W4246629945 creator A5013346012 @default.
- W4246629945 date "2001-04-15" @default.
- W4246629945 modified "2023-09-25" @default.
- W4246629945 title "1,3-Dihydrobenzo[c]thiophene 2,2-Dioxide" @default.
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- W4246629945 doi "https://doi.org/10.1002/047084289x.rd225" @default.
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