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- W4247155406 abstract "The behaviour of a graphite based thin mercury film electrode (TMFE) prepared “in situ” and a HMDE taken as a model electrode applying cyclic and stripping voltammetry was compared. In this comparison the useful potential ranges, the residual currents, the cyclic curves for hydroquinone, nitrobenzene, iodate, Fe(C2O4)33−, Cd2+, Pb2+, Cu2+ and Zn2+ ions as well as the stripping curves for Cd, Pb and Cu were studied. The experimental results obtained for amalgam forming metals were also compared with the rigorous voltammetric theory given by de Vries and van Dalen. Under conditions where the solubilities of the metals investigated in mercury were not exceeded a very good agreement between experiments and theory was obtained for the shifts of cathodic and anodic peak potentials and for the width of the anodic peak at half height (b1/2) as well as for relationship between anodic peak current and the rate of potential scan, deposition time and concentration of metal ions in the solution. With increasing excess of metal in mercury film over the value given by solubility data the agreement between experimental and theoretical results began to fail." @default.
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- W4247155406 date "1976-12-25" @default.
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- W4247155406 title "Cyclic and stripping voltammetry with graphite based thin mercury film electrodes prepared “in situ”" @default.
- W4247155406 doi "https://doi.org/10.1016/0368-1874(76)87002-5" @default.
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