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- W4247363039 abstract "In part I, Timm and Rachow (1) describe an algorithm for interpretation of chromatograms for imperfect resolution. The instrument was one of low plate counts, and yet population density distributions consistent with theoretical, kinetic models were achieved (2,3). Research, using high plate count columns, shows that convergent distributions are achieved and that results are not a function of instrument resolution. Linear polystyrene resins had a polydispersity in the interval 1.5 < Mw/Mn< 2.0. Data analysis includes mass fractions of unreacted monomers and species of similar molecular weight. A second algorithm is described for analysis of resins of narrow, molecular distributions Mw/Mn ≈ 1.0. Experimental testing incorporates polystyrene initiated with n-butyl lithium and a linear, step-growth epoxy comprised of nadic methyl anhydride and phenyl glycidyl ether. Kinetic distributions are described by a Poisson molar distribution. The accuracy of experimental population density distributions for macromolecular species is observed to be limited by" @default.
- W4247363039 created "2022-05-12" @default.
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- W4247363039 date "1984-03-30" @default.
- W4247363039 modified "2023-09-26" @default.
- W4247363039 title "Gel Permeation Chromatography" @default.
- W4247363039 doi "https://doi.org/10.1021/bk-1984-0245.ch007" @default.
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