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- W4247658002 abstract "Phenylated cyclopentasilanes Si5Ph10-nXn (X = H, F, CI, Br, I; n = 1, 2) have been prepared by dearylation of Si5Ph10 with triflic acid. Disubstitution gives high yields of the trans-1,3-isomer. The crystal structure of trans-1,3-difluorooctaphenylcyclopentasilane has been determined. Triflation of the novel educt (p-TolSiPh)4 for the first time allows the selective monofunctionalization of a perarylated cyclotetrasilane. The synthesized compounds have been characterized by 29Si, 19F, and 1H NMR spectroscopy (including Si-Si coupling constants) and will be used for the preparation of mixed halogenated cyclosilanes as well as for further NMR studies." @default.
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- W4247658002 date "2005-07-26" @default.
- W4247658002 modified "2023-10-03" @default.
- W4247658002 title "Synthesis, Reactivity, and Spectroscopy of Phenylated Cyclotetrasilanes and Cyclopentasilanes" @default.
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- W4247658002 doi "https://doi.org/10.1002/9783527620777.ch17a" @default.
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