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- W4247827737 abstract "1-(p-Methoxyphenyl)-3, 5-dimethyl-3-azabicyclo [3. 3. 1] nonane-⊿9, α-acetaldehyde was synthesized from 1-(p-methoxyphenyl)-3, 5-dimethyl-3-azabicyclo [3. 3. 1] nonan-9-one (VI) by reaction with ethoxyethynyllithium and partial hydrogenation of the ethoxyethynyl carbinol (IX) followed by treatment with phosphorus tribromide. This α, β-unsaturated aldehyde would be a suitable starting material for the synthesis of diterpenoid alkaloids, because cyclization of a derivative having a tertiary hydroxyl group at C-9 position of the phenylazabicyclononane did not form an expected compound." @default.
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- W4247827737 date "1963-01-01" @default.
- W4247827737 modified "2023-09-26" @default.
- W4247827737 title "An Approach to Synthesis of Diterpenoid Alkaloids. III." @default.
- W4247827737 doi "https://doi.org/10.1248/cpb.11.770" @default.
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