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- W4248769413 abstract "Imidazole and pyrazole reacts with diethyltin(IV) dihalides to yield adducts of the type Et2SnX2L2 (X Cl, Br). The structure of dibromobis(pyrazole)diethyltin(IV) has been determined by X-ray diffraction. (Crystal data: C10H18Br2N4Sn, M = 472.79, monoclinic, C2/c, a 1426.6(3), b 888.4(1) c 1393.9(6) pm, β 114.83(3)°, V 1603.3 × 106 pm3, Z = 4, R = 0.035). The crystal consists of discrete trans-SnEt2Br2(HPz)2 units with the metal atom octahedrally coordinated to two Br atoms (SnBr: 274.6(1) pm, BrSnBr: 180°), two ethyl carbons (SnC: 209.3(7) pm, CSnC: 180°), and two pyrazole groups (SnN: 235.6(4) pm, NSnN: 180°). The pyrazole ligands are intramolecularly and intermolecularly hydrogen bonded to the bromine atoms. The IR data are consistent with this trans-stereo-chemistry for all the compounds prepared. The 1H NMR data indicate that the pyrazole compounds dissociate fully in DMSO-d6 and partially in CDCl3." @default.
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- W4248769413 date "1988-09-01" @default.
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- W4248769413 title "Complexes of diethyldihalotin (IV) with imidazole and pyrazole. The crystal structure of dibromobis (pyrazole) diethyltin (IV)" @default.
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- W4248769413 doi "https://doi.org/10.1016/0022-328x(88)83060-2" @default.
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