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- W4248983907 abstract "The structure of the orthorhombic room-temperature phase of Cu(8)GeS(6) (copper germanium sulfide), M(r) = 773.27, has been refined on the basis of X-ray diffraction data from a 12-fold twinned crystal applying a six-dimensional twin refinement technique. For 1804 unique reflections measured using Mo Kalpha radiation, R(F) was 0.083 with 77 structure parameters and 12 scale factors. The symmetry operations, the unit cell and other crystal data are (0, 0, 0; (1/2), (1/2), 0) + x, y, z; y, x, z; (1/4) - x, (3/4) - y, (1/2) + z; (3/4) - y, (1/4) - x, (1/2) + z; a = b = 9.9073 (3) Å, c = 9.8703 (4) Å, alpha = beta = 90 degrees, gamma = 90.642 (4) degrees; V = 968.7 (1) Å(3), Z = 4, D(x) = 5.358 Mg m(-3), µ = 21.70 mm(-1). The standard setting of the space group and the reduced unit cell are Pmn2(1); a = 7.0445 (3), b = 6.9661 (3), c = 9.8699 (5) Å; Z = 2." @default.
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- W4248983907 date "1999-10-01" @default.
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- W4248983907 title "Structure refinement of Cu<sub>8</sub>GeS<sub>6</sub> using X-ray diffraction data from a multiple-twinned crystal" @default.
- W4248983907 doi "https://doi.org/10.1107/s0108768199004541" @default.
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