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- W4254332258 abstract "Abstract The crystal structure of [MgCl 2 (HCOOC 2 H 5 ) 2 ] 3 , obtained by slow crystallization at room temperature from a solution of α -MgCl 2 in dry ethyl formate, has been determined by X-ray diffraction. The structure was solved by direct and Fourier methods and refined by least-squares technique. This polymeric adduct is formed by asymmetric units having the formula [MgCl 2 (HCOOC 2 H 5 ) 2 ] 3 and crystallizes in an orthorhombic cell, space group Pbca (no. 61), a = 20.96(2) Å, b = 37.02(2) Å, c = 9.518(4) Å, V = 7385(8) Å 3 , Z = 8 and d c = 1.31 g cm −3 . The crystalline adduct consists of double-chloro bridged chain polymers in which the magnesium atom is nearly octahedrically coordinated by four chloro atoms and by the carbonyl oxygen atoms of two HCOOC 2 H 5 moieties, which are characterized by a marked crystallographic disorder. The octahedra share two edges by two double-chloro bridges between the magnesium atoms. There are only weak van der Waals interactions among the chains." @default.
- W4254332258 created "2022-05-12" @default.
- W4254332258 date "1992-02-01" @default.
- W4254332258 modified "2023-09-26" @default.
- W4254332258 title "Crystal structure of a magnesium chloride-ethylformate adduct" @default.
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- W4254332258 doi "https://doi.org/10.1524/zkri.1992.201.3-4.161" @default.
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