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- W4254662178 abstract "Preliminary results on the synthesis and characterization of anisotropic networks, oriented on a macroscopic scale, are reported. Fiber samples of segmented thermotropic liquid-crystalline polymers bearing the oxypentenyl lateral substituent have been crosslinked via thermally activated radical reaction. This was made possible by immersion of fiber samples in dichloromethane containing t-butylperoxybenzoate as activating agent, thus allowing its diffusion in the samples. Subsequent annealing at 145°C brings us to an anisotropic network with no loss of the original orientation. A mesophase is stabilized and no structural modification is observed by heating samples from room temperature up to 400°C, where thermal decomposition takes place. Crosslinked fibers exhibit good tensile properties, at both room temperature and at 150°C. © 1998 John Wiley & Sons, Inc. J Polym Sci B: Polym Phys 36: 433–438, 1998" @default.
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- W4254662178 date "1998-02-01" @default.
- W4254662178 modified "2023-09-28" @default.
- W4254662178 title "Crosslinking of a fibrous sample to a macro‐oriented mesomorphic network" @default.
- W4254662178 doi "https://doi.org/10.1002/(sici)1099-0488(199802)36:3<433::aid-polb5>3.3.co;2-e" @default.
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