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- W4255175095 abstract "Methyl 4,6-di-O-p-toluenesulfonyl-α-D-threo-hex-2-enopyranoside 4b reacts with methylamine at room temperature to displace the allylic sulfonate only, and the ethyl urethane of the resulting 4-N-methylamino sugar is cyclized with iodonium ion to give the 2-iodo-oxazolidinone, 13. This substance, upon treatment with sodium iodide in acetone, gives the 2,6-diiodide 14a. Deiodination, followed by base hydrolysis, gives the cis-hydroxyamino precursor, which upon N-acetylation and O-methylation affords the previously known holacosaminide 1b." @default.
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- W4255175095 date "1984-08-01" @default.
- W4255175095 modified "2023-10-12" @default.
- W4255175095 title "Stereocontrolled routes to <i>cis</i>-hydroxyamino sugars. Part VII. A synthesis of holacosamine" @default.
- W4255175095 doi "https://doi.org/10.1139/v84-262" @default.
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