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- W4256594893 abstract "Highly reactive calcium can be readily prepared by the reduction of calcium halides in tetrahydrofuran (THF) solution with preformed lithium biphenylide under an argon atmosphere at room temperature. This colored calcium species seems to be reasonably soluble in THF. However, the reactive calcium complex prepared from preformed lithium naphthalenide was insoluble in THF solution and precipitated out of solution to give a highly reactive black solid. Highly reactive calcium was prepared by the lithium biphenylide reduction of calcium salts in THF. The organocalcium compounds prepared directly from this calcium complex and organic halides were found to efficiently undergo Grignard-type reactions. A highly reactive form of calcium has been prepared by the lithium biphenylide or lithium naphthalenide reduction of calcium salts. This calcium will rapidly undergo an effective oxidative addition reaction with alkyl or aryl halides to yield the corresponding organocalcium compounds." @default.
- W4256594893 created "2022-05-12" @default.
- W4256594893 date "2016-11-18" @default.
- W4256594893 modified "2023-10-16" @default.
- W4256594893 title "Calcium" @default.
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- W4256594893 doi "https://doi.org/10.1002/9781118929124.ch9" @default.
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