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- W4256597072 abstract "1,1-Dimethyl-1-(2-hydroxypropyl)amine p-substituted benzimide (“aminimide”) derivatives were prepared by the reaction of p-substituted methyl benzoates with equimolar amounts of 1,1-dimethylhydrazine and propylene oxide. These ylide compounds are shown to be useful as thermally latent initiators for the polymerization of glycidyl phenyl ether (GPE). Bulk polymerization of GPE with 3 mol % of these aminimides was carried out at 40–150°C for 8 h, showing ≥ 100°C was required for an effective rate. No consumption of the monomer could be observed at temperatures lower than 80°C. p-Methoxy substituted 1 showed the largest thermal latency among four aminimides tested. The activities of the aminimides increased with an increase of electron-donating ability of the substituents on the benzene ring, according to the following order: 1 (p-MeO) > 2(p-Me) > 3(H) > 4(p-NO2). © 1997 John Wiley & Sons, Inc. J Polym Sci A: Polym Chem 35: 689–694, 1997" @default.
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- W4256597072 date "1997-03-01" @default.
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- W4256597072 title "Thermal latency and structure‐activity relationship of aminimides in the polymerization of epoxide" @default.
- W4256597072 doi "https://doi.org/10.1002/(sici)1099-0518(199703)35:4<689::aid-pola11>3.3.co;2-n" @default.
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