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- W4280490590 abstract "Electrochemical synthesis of versatile β-keto sulfonyl fluorides is accomplished by radical fluorosulfonylation of vinyl triflates with FSO2Cl as the fluorosulfonyl radical source. This electroreductive protocol uses inexpensive graphite felt as electrodes, thus avoiding the use of a sacrificial anode. Moreover, this protocol, featuring metal-free, mild conditions and easy scalability, allows expedient access to valuable β-keto sulfonyl fluorides from readily available precursors, as well as the cyclic ones that are otherwise inaccessible using prior methods." @default.
- W4280490590 created "2022-05-22" @default.
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- W4280490590 date "2022-05-17" @default.
- W4280490590 modified "2023-10-02" @default.
- W4280490590 title "Electrochemical Synthesis of β-Keto Sulfonyl Fluorides via Radical Fluorosulfonylation of Vinyl Triflates" @default.
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- W4280490590 doi "https://doi.org/10.1021/acs.orglett.2c01336" @default.
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