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- W4280492056 endingPage "111961" @default.
- W4280492056 startingPage "111961" @default.
- W4280492056 abstract "Nanoparticles, such as noble metal nanoparticles and covalent organic frameworks (COFs), advance heterogeneous catalysis. Three COFs were synthesized via the solvothermal method using tricarboxylic acids (tricarboxylic benzene (2,4,6-tri-p-carboxyphenylpyridine (H 3 L2), 4,4′,4''-tri carboxyl triphenylamine (H 3 L1), and trimesic acid (H 3 BTC)) and 1,3,5-triazine-2,4,6-triamine moieties. The synthesized COFs were potentially used as supports for the in-situ growth of palladium nanocrystals (Pd NCs), offering a particle size of 1–5 nm. X-ray diffraction (XRD), Fourier transforms infrared (FT-IR), transmission electron microscopy (TEM), high-resolution TEM (HR-TEM), nitrogen adsorption-desorption isotherms, thermogravimetric analysis (TGA), and X-ray photoelectron spectroscopy (XPS) characterized the materials. Using Heck cross-coupling reaction, Pd NCs@COFs were used as catalysts to synthesize different organic molecules via carbon-carbon (C–C) formation. They exhibit complete conversion (100%) for vinyl derivatives and aryl halides (Bromo- and Chloro-derivatives) with good stability. Pd NCs@COFs maintain high catalytic activity over four consecutive cycles. • Synthesis of two new Covalent organic frameworks (COFs). • In-situ growth of palladium nanocrystals into COFs. • Applications of Pd NCs@COFs for C–C cross-coupling reactions via Heck Reaction. • Record high heterogeneous catalytic performance of the prepared catalysts." @default.
- W4280492056 created "2022-05-22" @default.
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- W4280492056 date "2022-07-01" @default.
- W4280492056 modified "2023-09-29" @default.
- W4280492056 title "Palladium nanocrystals-embedded covalent organic framework as an efficient catalyst for Heck cross-coupling reaction" @default.
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- W4280492056 doi "https://doi.org/10.1016/j.micromeso.2022.111961" @default.
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