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• W4280493982 abstract "Abstract Colourless single crystals of Ge(SO 4 ) 2 were obtained as single phase products from the binary oxides GeO 2 and SO 3 . The reaction was carried out in a silica glass ampule enclosed in an autoclave at 350 °C. Ge(SO 4 ) 2 forms a layer structure with corner‐linked GeO 6 octahedra and SO 4 tetrahedra. The crystal structure ( R c , Z =6, a =4.622 Å, c =42.576 Å) belongs to the Ni(ClO 4 ) 2 ‐type. The SO 4 tetrahedra are rotated by 24°. The sense of rotation alternates between adjacent layers. This rotation is connected to a super structure with a doubled c ‐axis and a disorder between the layers according to the sense of rotation. Ge(SO 4 ) 2 is one of the very rare examples of a sulphate of a tetravalent cation and is the representative with the smallest ionic radius. Lattice energy calculations confirm the electrostatic consistency. Vibrational spectra were recorded and show the typical features of GeO 6 and SO 4 units." @default.
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• W4280493982 date "2022-05-12" @default.
• W4280493982 modified "2023-09-30" @default.
• W4280493982 title "Synthesis and crystal structure of Ge(SO₄)₂" @default.
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• W4280493982 doi "https://doi.org/10.1002/zaac.202200079" @default.
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