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- W4280494038 abstract "Carbohydrate-based oxepines are seven-membered-ring oxacycles containing an enol ether moiety. These compounds have been used as intermediates in the preparation of septanose carbohydrates by functionalization through their double bond. Reported here is a new synthesis of a carbohydrate based oxepine that uses 2,3;4,6-di-O-acetonide mannose as a key starting material. The oxepine is an important precursor used in the synthesis of septanose glycomimetics of mannopyranosides. The central feature of the synthesis is a two-step sequence that converts a septanose 1,2-di-O-acetate to the septanosyl bromide and onward to the oxepine via a reductive elimination." @default.
- W4280494038 created "2022-05-22" @default.
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- W4280494038 date "2022-05-16" @default.
- W4280494038 modified "2023-10-02" @default.
- W4280494038 title "Synthesis of a Diacetonide-Protected, Mannose-Based Oxepine: Configurational Control of Anomeric Acetate Activation" @default.
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- W4280494038 doi "https://doi.org/10.1021/acs.joc.2c00206" @default.
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