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- W4280494068 abstract "An efficient palladium-catalyzed electrooxidation C–H acylation reaction of N -nitrosoanilines with α -oxocarboxylic acids was developed. The anodic oxidation of the Pd(II) intermediate was found to be the key to complete the reaction. In this case, the N -nitroso group was observed to be an effective directing group for C–H activation reaction. Moreover, the synthetic transformation of derivatives of natural products (L-menthol, dehydroepiandrosterone, and pregnenolone) was successfully realized. Finally, flow electrochemical synthesis of some substrates was achieved. An efficient palladium-catalyzed electrooxidation C–H acylation reaction of N -nitrosoanilines with α -oxocarboxylic acids was developed." @default.
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- W4280494068 date "2023-02-01" @default.
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- W4280494068 title "Electrochemically mediated decarboxylative acylation of N-nitrosoanilines with α-oxocarboxylic acids" @default.
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- W4280494068 doi "https://doi.org/10.1016/j.cclet.2022.05.051" @default.
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