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- W4280498949 abstract "Abstract Key steps in the synthesis of derivatives of the angucycline, tetrangulol include the use of a palladium catalyzed Suzuki‐Miyaura cross‐coupling reaction for the assembly of 2‐(1,4‐dimethoxy‐3‐(2‐methylprop‐1‐en‐1‐yl)naphthalen‐2‐yl)‐3‐methoxy‐5‐methylbenzaldehyde from 2‐iodo‐3‐methoxy‐5‐methylbenzaldehyde and 2‐(1,4‐dimethoxy‐3‐(2‐methylprop‐1‐en‐1‐yl)naphthalen‐2‐yl)‐4,4,5,5‐tetramethyl‐1,3,2‐dioxaborolane. The biaryl product was then subjected to an iron‐catalyzed ring‐closing carbonyl‐olefin metathesis reaction to afford 1,7,12‐trimethoxy‐3‐methyltetraphene, which was oxidized to the corresponding quinone. Late stage oxidation of the quinone with Ru[Cl 2 ( p ‐cymene)] 2 and an oxidant unexpectedly afforded the chlorinated compounds, 2,4‐dichloro‐11‐hydroxy‐1‐methoxy‐3‐methyltetraphene‐7,12‐dione and 2,4‐dichloro‐6‐hydroxy‐1‐methoxy‐3‐methyltetraphene‐7,12‐dione." @default.
- W4280498949 created "2022-05-22" @default.
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- W4280498949 date "2022-06-21" @default.
- W4280498949 modified "2023-09-27" @default.
- W4280498949 title "Synthesis of Angucycline/Tetrangulol Derivatives Using Suzuki‐Miyaura Cross‐Coupling and Ring‐Closing Carbonyl–Olefin Metathesis Reactions" @default.
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- W4280498949 doi "https://doi.org/10.1002/ejoc.202200348" @default.
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