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• W4281490464 abstract "While the N-trifluoromethylation of cyclic ureas is of interest for the potential to fundamentally change the properties of these biologically relevant moieties, the single synthetic procedure known to date describing their access only gives 4,4-disubstituted or fused aromatic cyclic N-CF3 urea derivatives. We herein report an alternative approach to unleash access to the 4-monosubstituted imidazolidinone motif. The strategy relies on straightforward cyclization of readily accessible acyclic ureas, enabled by Ag-catalysis or light-assisted proton coupled electron transfer. The cyclic core is shown to be highly robust and amenable to various derivatizations, such as tandem Ni-catalysis, C-B, C-N, C-C cross couplings or C-H functionalizations, tolerating basic, nucleophilic and/or oxidizing conditions." @default.
• W4281490464 created "2022-05-26" @default.
• W4281490464 creator A5042568607 @default.
• W4281490464 creator A5047300640 @default.
• W4281490464 creator A5072784520 @default.
• W4281490464 date "2022-06-24" @default.
• W4281490464 modified "2023-10-14" @default.
• W4281490464 title "<i>N</i>‐CF₃ Imidazolidin‐2‐one Derivatives via Photocatalytic and Silver‐Catalyzed Cyclizations" @default.
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• W4281490464 doi "https://doi.org/10.1002/chem.202201435" @default.
• W4281490464 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/35611709" @default.
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