Matches in SemOpenAlex for { <https://semopenalex.org/work/W4281664878> ?p ?o ?g. }
Showing items 1 to 92 of
92
with 100 items per page.
- W4281664878 endingPage "5051" @default.
- W4281664878 startingPage "5043" @default.
- W4281664878 abstract "Centrifugal partition chromatography (CPC) and countercurrent chromatography (CCC) are two preparative techniques mainly used for the isolation and purification of natural products. While CPC benefits from a larger sample capacity, CCC typically provides better peak resolutions and hereby higher purities. In this study, we aimed to combine both advantages by the direct linking of CPC and CCC which was achieved by installation of switching valves and connection tube. The hyphenated CPC-CCC setup was tested with major alkylresorcinols which were obtained from a transesterified and hydrogenated rye extract. Injections of 1- and 5-g samples into the individual CCC system confirmed the limited sample capacity because of immediate flooding with the 5-g sample (total loss of stationary phase). In comparison, the CPC system was stable with 5- and 10-g samples but the peak resolution with 1-g sample was poorer than with the CCC system. Injections of 5- and 10-g samples into the CPC-CCC system were successful. However, a sample load of 10 g resulted in lower purities of the alkylresorcinols (80% or less) due to peak tailing. By contrast, injection of 5-g sample provided high amounts of ~ 1.2 g alkylresorcinols with purities of > 95%." @default.
- W4281664878 created "2022-06-13" @default.
- W4281664878 creator A5005450343 @default.
- W4281664878 creator A5067095972 @default.
- W4281664878 date "2022-05-31" @default.
- W4281664878 modified "2023-10-14" @default.
- W4281664878 title "Online hyphenation of centrifugal partition chromatography with countercurrent chromatography (CPC-CCC) and its application to the separation of saturated alkylresorcinols" @default.
- W4281664878 cites W1964295420 @default.
- W4281664878 cites W1981636492 @default.
- W4281664878 cites W1987135617 @default.
- W4281664878 cites W1998633981 @default.
- W4281664878 cites W1999737354 @default.
- W4281664878 cites W2014244092 @default.
- W4281664878 cites W2018592925 @default.
- W4281664878 cites W2023096161 @default.
- W4281664878 cites W2039532183 @default.
- W4281664878 cites W2042010437 @default.
- W4281664878 cites W2059517978 @default.
- W4281664878 cites W2084505217 @default.
- W4281664878 cites W2086801771 @default.
- W4281664878 cites W2092239865 @default.
- W4281664878 cites W2094699931 @default.
- W4281664878 cites W2162807335 @default.
- W4281664878 cites W2326761961 @default.
- W4281664878 cites W2335884626 @default.
- W4281664878 cites W2419303101 @default.
- W4281664878 cites W2469374716 @default.
- W4281664878 cites W2519094979 @default.
- W4281664878 cites W2585988805 @default.
- W4281664878 cites W2616460321 @default.
- W4281664878 cites W2790246079 @default.
- W4281664878 cites W2802621137 @default.
- W4281664878 cites W2918051138 @default.
- W4281664878 cites W2921991626 @default.
- W4281664878 cites W2964220702 @default.
- W4281664878 cites W3091798853 @default.
- W4281664878 cites W3133848390 @default.
- W4281664878 cites W3213045884 @default.
- W4281664878 cites W4210976592 @default.
- W4281664878 cites W927558366 @default.
- W4281664878 doi "https://doi.org/10.1007/s00216-022-04136-x" @default.
- W4281664878 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/35639138" @default.
- W4281664878 hasPublicationYear "2022" @default.
- W4281664878 type Work @default.
- W4281664878 citedByCount "4" @default.
- W4281664878 countsByYear W42816648782022 @default.
- W4281664878 countsByYear W42816648782023 @default.
- W4281664878 crossrefType "journal-article" @default.
- W4281664878 hasAuthorship W4281664878A5005450343 @default.
- W4281664878 hasAuthorship W4281664878A5067095972 @default.
- W4281664878 hasBestOaLocation W42816648781 @default.
- W4281664878 hasConcept C113196181 @default.
- W4281664878 hasConcept C138268822 @default.
- W4281664878 hasConcept C154945302 @default.
- W4281664878 hasConcept C185592680 @default.
- W4281664878 hasConcept C2778576202 @default.
- W4281664878 hasConcept C41008148 @default.
- W4281664878 hasConcept C43617362 @default.
- W4281664878 hasConcept C51724486 @default.
- W4281664878 hasConcept C63258622 @default.
- W4281664878 hasConceptScore W4281664878C113196181 @default.
- W4281664878 hasConceptScore W4281664878C138268822 @default.
- W4281664878 hasConceptScore W4281664878C154945302 @default.
- W4281664878 hasConceptScore W4281664878C185592680 @default.
- W4281664878 hasConceptScore W4281664878C2778576202 @default.
- W4281664878 hasConceptScore W4281664878C41008148 @default.
- W4281664878 hasConceptScore W4281664878C43617362 @default.
- W4281664878 hasConceptScore W4281664878C51724486 @default.
- W4281664878 hasConceptScore W4281664878C63258622 @default.
- W4281664878 hasFunder F4320311402 @default.
- W4281664878 hasIssue "17" @default.
- W4281664878 hasLocation W42816648781 @default.
- W4281664878 hasLocation W42816648782 @default.
- W4281664878 hasLocation W42816648783 @default.
- W4281664878 hasOpenAccess W4281664878 @default.
- W4281664878 hasPrimaryLocation W42816648781 @default.
- W4281664878 hasRelatedWork W2003302128 @default.
- W4281664878 hasRelatedWork W2018816110 @default.
- W4281664878 hasRelatedWork W2024454492 @default.
- W4281664878 hasRelatedWork W2042124022 @default.
- W4281664878 hasRelatedWork W2052789144 @default.
- W4281664878 hasRelatedWork W2075935640 @default.
- W4281664878 hasRelatedWork W2461902583 @default.
- W4281664878 hasRelatedWork W2473988186 @default.
- W4281664878 hasRelatedWork W2573693990 @default.
- W4281664878 hasRelatedWork W89894663 @default.
- W4281664878 hasVolume "414" @default.
- W4281664878 isParatext "false" @default.
- W4281664878 isRetracted "false" @default.
- W4281664878 workType "article" @default.