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- W4281701516 abstract "A tandem semipinacol rearrangement/aldehyde arylation or alkylation reaction leading to formation of functionalized 1,3-diols bearing three consecutive tertiary stereocenters is identified from the reaction of various new trisubstituted 2,3-epoxy alcohols with numerous Grignard reagents. This reaction is useful for stereoselective construction of three consecutive tertiary stereocenters. The observed 1,3-diols exist in the anti configuration, which is confirmed by two-dimensional nuclear Overhauser effect spectroscopy, the crystal structure of acetonide of 1,3-diol analogue 3ai, and further density functional theory studies." @default.
- W4281701516 created "2022-06-13" @default.
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- W4281701516 date "2022-06-09" @default.
- W4281701516 modified "2023-10-12" @default.
- W4281701516 title "A Tandem Semipinacol Rearrangement/Aldehyde Arylation or Alkylation of Trisubstituted 2,3-Epoxy Alcohols with Grignard Reagents for Functionalized 1,3-Diols" @default.
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- W4281701516 doi "https://doi.org/10.1021/acs.joc.2c00267" @default.
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