Matches in SemOpenAlex for { <https://semopenalex.org/work/W4283379392> ?p ?o ?g. }
Showing items 1 to 91 of
91
with 100 items per page.
- W4283379392 endingPage "2627" @default.
- W4283379392 startingPage "2620" @default.
- W4283379392 abstract "A flame retardant with abundant phosphorus-nitrogen content and a highly symmetric structure, 3,9-bis(phenyl(phenylamino)methyl)-2,4,8,10-tetraoxa-3,9-diphosphaspiro[5.5]undecane 3,9-dioxide (BTDD), was synthesized by the reaction of 2,4,8,10-tetraoxa-3,9-diphosphaspiro[5.5]undecane 3,9-dioxide (DHDP) with Schiff base (2-(N-phenyliminomethyl)phenol) (NDPA). The structure of BTDD was characterized by nuclear magnetic resonance (1H NMR and 31P NMR) and Fourier transform infrared (FT-IR) spectroscopy. Its thermal stability was characterized by thermogravimetric analysis (TGA). The solubilities of BTDD in acetonitrile, acetone, tetrahydrofuran, benzene, ethanol, isopropanol, 1,4-dioxane, 1,2-dichloroethane, toluene, diethyl ether, dichloromethane, and acetic acid were determined with the static gravimetric method at temperatures ranging from 283.15 to 343.15 K. The results showed that the dissolution behavior of BTDD in tetrahydrofuran and toluene was more prominent. The solubilities of BTDD in the 12 solvents were positively correlated with temperature, and the solubility order from high to low is tetrahydrofuran, toluene, dichloromethane, 1,2-dichloroethane, isopropanol, (diethyl ether, 1,4-dioxane), acetic acid, acetone, benzene (ethanol, acetonitrile). The modified Apelblat thermodynamic model was used to correlate the measured solubility data, which shows good consistency with the experimental values. In all measurements, the root-mean-square deviation was less than 0.1%, and the average relative error was less than 0.04." @default.
- W4283379392 created "2022-06-25" @default.
- W4283379392 creator A5007800588 @default.
- W4283379392 creator A5032005332 @default.
- W4283379392 creator A5041615492 @default.
- W4283379392 creator A5074614470 @default.
- W4283379392 creator A5078226849 @default.
- W4283379392 creator A5085845614 @default.
- W4283379392 date "2022-06-24" @default.
- W4283379392 modified "2023-09-25" @default.
- W4283379392 title "Solubility Determination and Data Correlation of a New Flame Retardant 3,9-Bis(phenyl(phenylamino)methyl)-2,4,8,10-tetraoxa-3,9-diphosphaspiro [5.5] undecane 3,9-dioxide in 12 Pure Solvents from 283.15 to 343.15 K" @default.
- W4283379392 cites W1971713833 @default.
- W4283379392 cites W2060482516 @default.
- W4283379392 cites W2146629248 @default.
- W4283379392 cites W2289023954 @default.
- W4283379392 cites W2330171922 @default.
- W4283379392 cites W2487391883 @default.
- W4283379392 cites W2553543101 @default.
- W4283379392 cites W2587487669 @default.
- W4283379392 cites W2767615168 @default.
- W4283379392 cites W2767925551 @default.
- W4283379392 cites W2771542465 @default.
- W4283379392 cites W2786993001 @default.
- W4283379392 cites W2895078393 @default.
- W4283379392 cites W2916387779 @default.
- W4283379392 cites W2924499744 @default.
- W4283379392 cites W2970222036 @default.
- W4283379392 cites W3005425101 @default.
- W4283379392 cites W3009047849 @default.
- W4283379392 cites W3037399661 @default.
- W4283379392 cites W3134856807 @default.
- W4283379392 cites W3157098634 @default.
- W4283379392 cites W3172172548 @default.
- W4283379392 doi "https://doi.org/10.1021/acs.jced.2c00044" @default.
- W4283379392 hasPublicationYear "2022" @default.
- W4283379392 type Work @default.
- W4283379392 citedByCount "0" @default.
- W4283379392 crossrefType "journal-article" @default.
- W4283379392 hasAuthorship W4283379392A5007800588 @default.
- W4283379392 hasAuthorship W4283379392A5032005332 @default.
- W4283379392 hasAuthorship W4283379392A5041615492 @default.
- W4283379392 hasAuthorship W4283379392A5074614470 @default.
- W4283379392 hasAuthorship W4283379392A5078226849 @default.
- W4283379392 hasAuthorship W4283379392A5085845614 @default.
- W4283379392 hasConcept C13965031 @default.
- W4283379392 hasConcept C155574463 @default.
- W4283379392 hasConcept C178790620 @default.
- W4283379392 hasConcept C185592680 @default.
- W4283379392 hasConcept C2776445513 @default.
- W4283379392 hasConcept C2776701986 @default.
- W4283379392 hasConcept C2776721371 @default.
- W4283379392 hasConcept C2777463227 @default.
- W4283379392 hasConcept C2777691172 @default.
- W4283379392 hasConcept C2778142098 @default.
- W4283379392 hasConcept C2780400988 @default.
- W4283379392 hasConcept C2780471494 @default.
- W4283379392 hasConcept C2781213060 @default.
- W4283379392 hasConceptScore W4283379392C13965031 @default.
- W4283379392 hasConceptScore W4283379392C155574463 @default.
- W4283379392 hasConceptScore W4283379392C178790620 @default.
- W4283379392 hasConceptScore W4283379392C185592680 @default.
- W4283379392 hasConceptScore W4283379392C2776445513 @default.
- W4283379392 hasConceptScore W4283379392C2776701986 @default.
- W4283379392 hasConceptScore W4283379392C2776721371 @default.
- W4283379392 hasConceptScore W4283379392C2777463227 @default.
- W4283379392 hasConceptScore W4283379392C2777691172 @default.
- W4283379392 hasConceptScore W4283379392C2778142098 @default.
- W4283379392 hasConceptScore W4283379392C2780400988 @default.
- W4283379392 hasConceptScore W4283379392C2780471494 @default.
- W4283379392 hasConceptScore W4283379392C2781213060 @default.
- W4283379392 hasFunder F4320322868 @default.
- W4283379392 hasIssue "9" @default.
- W4283379392 hasLocation W42833793921 @default.
- W4283379392 hasOpenAccess W4283379392 @default.
- W4283379392 hasPrimaryLocation W42833793921 @default.
- W4283379392 hasRelatedWork W1969507540 @default.
- W4283379392 hasRelatedWork W1970991182 @default.
- W4283379392 hasRelatedWork W2043899894 @default.
- W4283379392 hasRelatedWork W2125111755 @default.
- W4283379392 hasRelatedWork W2490715155 @default.
- W4283379392 hasRelatedWork W2972626238 @default.
- W4283379392 hasRelatedWork W2977687700 @default.
- W4283379392 hasRelatedWork W3037985277 @default.
- W4283379392 hasRelatedWork W3157642071 @default.
- W4283379392 hasRelatedWork W4251304988 @default.
- W4283379392 hasVolume "67" @default.
- W4283379392 isParatext "false" @default.
- W4283379392 isRetracted "false" @default.
- W4283379392 workType "article" @default.