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- W4283586634 abstract "A simple and selective LC method is described for the determination of Netupitant and Palonosetron in tablet dosage forms. Chromatographic separation was achieved on a Inertsil ODS (C18) RP Column (250mm x 4.6 mm. 5µm) column using mobile phase consisting of a 55 volumes of mixed phosphate buffer and 45 volumes of acetonitrile were prepared with detection of 253nm. Linearity was observed in the range 25-125 µg/ml for Netupitant (r 2 =0.995) and 50-150 µg /ml for Palonosetron (r 2 =0.999) for the amount of drugs estimated by the proposed methods was in good agreement with the label claim. The proposed methods were validated. The accuracy of the methods was assessed by recovery studies at three different levels. Recovery experiments indicated the absence of interference from commonly encountered pharmaceutical additives. The method was found to be precise as indicated by the repeatability analysis, showing %RSD less than 2. All statistical data proves validity of the methods and can be used for routine analysis of pharmaceutical dosage form." @default.
- W4283586634 created "2022-06-28" @default.
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- W4283586634 date "2022-06-27" @default.
- W4283586634 modified "2023-09-26" @default.
- W4283586634 title "new UPLC method development and validation for simultaneous estimation of netiputant and palonosetron using bulk and pharmaceutical dosage form using UPLC" @default.
- W4283586634 doi "https://doi.org/10.53730/ijhs.v6ns6.9801" @default.
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