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• W4283706769 abstract "Carbonylation of m-xylylene diamine (XDA) with ethyl carbamate to produce m-xylylene dicarbamate (XDC), which is the crucial intermediate for the production of m-xylylene diisocyanate (XDI), over the hierarchical TS-1 (HTS-1) zeolite catalyst was studied. The catalysts were characterized by Brunauer-Emmett-Teller, X-ray diffraction, Fourier transform infrared spectroscopy, scanning electron microscopy, and temperature-programed desorption of ammonia techniques systematically. The results showed that the high performance of HTS-1 could be attributed to the weak acidity and high Vmeso/Vtotal ratio of the catalyst. Impacts of reaction time and reusage on the HTS-1 catalyst were also investigated. Under 6 h and 200 °C, XDA conversion could reach 100% with 88.5% XDC yield. Furthermore, partial loss of Ti active sites with Lewis acidity on the catalyst surface led to the decrease of XDC yield during recycling. Moreover, a possible reaction mechanism for the title reaction was primarily proposed." @default.
• W4283706769 created "2022-06-30" @default.
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• W4283706769 date "2022-06-28" @default.
• W4283706769 modified "2023-09-25" @default.
• W4283706769 title "Effective Synthesis of <i>m</i>-Xylylene Dicarbamate via Carbonylation of <i>m</i>-Xylylene Diamine with Ethyl Carbamate over Hierarchical TS-1 Catalysts" @default.
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• W4283706769 doi "https://doi.org/10.1021/acsomega.2c02535" @default.
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