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• W4283720848 abstract "The components of the title compound, [Ni(C10H24N4)(H2O)2]2[Ni(C10H24N4)(C27H24O9P3)2]·10H2O are two centrosymmetric [Ni(C10H24N4)(H2O)2]2+ dications, a centrosymmetric [Ni(C10H24N4)(C27H24O9P3)2]4- tetra-anion and five crystallographically unique water mol-ecules of crystallization. All of the nickel ions are coordinated by the four secondary N atoms of the macrocyclic cyclam ligands, which adopt the most energetically stable trans-III conformation, and the mutually trans O atoms of either water mol-ecules in the cations or the phospho-nate groups in the anion in a tetra-gonally distorted NiN4O2 octa-hedral coordination geometry. Strong O-H⋯O hydrogen bonds between the protonated and the non-protonated phospho-nate O atoms of neighboring anions result in the formation of layers oriented parallel to the bc plane, which are linked into a three-dimensional network by virtue of numerous N-H⋯O and O-H⋯O hydrogen bonds arising from the sec-NH groups of the macrocycles, phospho-nate O atoms and coordinated and non-coordinated water mol-ecules." @default.
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• W4283720848 date "2022-06-30" @default.
• W4283720848 modified "2023-09-26" @default.
• W4283720848 title "Synthesis and crystal structure of bis[<i>trans</i>-diaqua(1,4,8,11-tetraazacyclotetradecane-κ⁴ <i>N</i> ¹,<i>N</i> ⁴,<i>N</i> ⁸,<i>N</i> ¹¹)nickel(II)] <i>trans</i>-(1,4,8,11-tetraazacyclotetradecane-κ⁴ <i>N</i> ¹,<i>N</i> ⁴,<i>N</i> ⁸,<i>N</i> ¹¹)bis[4,4′,4′′-(1,3,5-trimethylbenzene-2,4,6-triyl)tris(hydrogen phenylphosphonato-κ<i>O</i>)]nickel(II) decahydrate" @default.
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• W4283720848 doi "https://doi.org/10.1107/s2056989022006624" @default.
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