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• W4285384068 abstract "• Covalent triazine frameworks bearing sulfonic acid-based ionic liquids are demonstrated. • The cheese-like macropore morphology of the catalyst is achieved. • Strong Brønsted acidity and high accessibility of acid sites impact the activity. • Synergistic catalytic system of catalyst-DMSO-microwave irradiation is established. • The catalyst can be reused 5 times without obvious loss of catalytic activity. A simple method is proposed for the fabrication of nitrogen-rich macroporous covalent triazine frameworks bearing sulfonic acid-based ionic liquids (MNCTF-[C 3 pyr][OTf], C 3 = Pr SO 3 H, pyr = pyridine group, OTf = SO 3 CF 3 ) by chemical bonding. The MNCTF-[C 3 pyr][OTf] exhibits higher 5–hydroxymethylfurfural (HMF) yield of 98.9% than commercially available solid acids (e.g., Amberlyst-15 and HY zeolite) in the microwave-assisted fructose dehydration in dimethyl sulfoxide (DMSO) solvent. The excellent catalytic performance of the MNCTF-[C 3 pyr][OTf] closely depends on the strong Brønsted acidity and cheese-like macropore morphology, which results in high accessibility of the substrates to the acid sites. Additionally, the synergistic effect of DMSO with MNCTF-[C 3 pyr][OTf] catalyst and microwave irradiation also provides a positive role in enhancing selectivity to HMF. The MNCTF-[C 3 pyr][OTf] can be reused for five times without leaching of acid sites. This work underlines the great potential of covalent triazine frameworks-based solid acids in biomass conversion." @default.
• W4285384068 created "2022-07-14" @default.
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• W4285384068 date "2022-11-01" @default.
• W4285384068 modified "2023-09-30" @default.
• W4285384068 title "Nitrogen-rich macroporous covalent triazine frameworks bearing sulfonic acid-based ionic liquids for microwave-assisted conversion of fructose to 5–hydroxymethylfurfural" @default.
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• W4285384068 doi "https://doi.org/10.1016/j.fuel.2022.125230" @default.
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