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- W4285890999 abstract "Submicron tungsten diboride (WB2) powder was successfully synthesized with the ratio of WO3:B4C:C = 2:1.1:5. The effects of carbon sources (carbon black or graphite) and heat treatment temperatures (1100, 1200, 1300 ℃) on the phase composition and microstructure of the as-synthesized WB2 powder samples were studied. The results showed that ultrafine WB2 powders with oxygen content of 1.65 wt% and 2.04 wt% were obtained by carbon black and graphite at 1300 ℃, respectively. The relatively density of the as-sintered WB2 samples achieve ~ 91 % and ~ 87 % without any kind of sintering additive after spark plasma sintering at 1500 °C under 30 MPa for 10 min. The formation mechanism of the WB2 powders synthesized by boro/carbothermal reduction was proposed and verified by thermodynamic calculation according to the phases present in the powder synthesized at different temperatures." @default.
- W4285890999 created "2022-07-20" @default.
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- W4285890999 date "2022-10-01" @default.
- W4285890999 modified "2023-09-27" @default.
- W4285890999 title "Preparation of tungsten diboride by a combination of boro/carbothermal reduction process and spark plasma sintering" @default.
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- W4285890999 doi "https://doi.org/10.1016/j.jeurceramsoc.2022.06.006" @default.
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