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• W4286945663 abstract "Abstract The industrial application of powder‐based catalytic electrodes is heavily restricted by powder shedding, inhibition of active sites, and poor long‐term stability. Herein, a porous titanium carbonitride (TiC 0.5 N 0.5 ) ceramic substrate with open straight finger‐like holes is first made by a simple approach of phase‐inversion tape‐casting and pressureless sintering, and then a Co x Ni 1‐ x P active layer is in situ formed by a hydrothermal technique and phosphorization to achieve integrated Co x Ni 1‐ x P/TiC 0.5 N 0.5 self‐supported ceramic electrodes. Electrochemical tests reveal that the optimized Co 0.9 Ni 0.1 P/TiC 0.5 N 0.5 electrode exhibits overpotentials of 76.5 and 79.8 mV at 10 mA cm −2 , Tafel slopes of 47.3 and 40.5 mV dec −1 , in 0.5 m H 2 SO 4 and 1 m KOH, respectively. Furthermore, its superior long‐term stability and resistance to corrosion can be achieved for more than 20 h in both media at 100 mA cm −2 . In addition, the Co 0.9 Ni 0.1 P/TiC 0.5 N 0.5 electrode has much better performance than Pt/C at high current density in neutral media. Density functional theory calculations confirm that the Ni substitution of 1/10 Co in CoP leads to the more optimal |Δ G H* | among the Co x Ni 1‐ x P catalysts. Compared with other CoP or NiP‐based electrodes, the Co 0.9 Ni 0.1 P/TiC 0.5 N 0.5 electrode benefits from high strength, unique pore structure, tight and compatible bonding, and high hydrophilicity." @default.
• W4286945663 created "2022-07-25" @default.
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• W4286945663 date "2022-07-24" @default.
• W4286945663 modified "2023-09-26" @default.
• W4286945663 title "Electrocatalytic Self‐Supported‐Electrode Based on Co<i>_x</i>Ni_1‐<i>_x</i>P/TiC_0.5N_0.5 for Enhancing pH‐Universal Hydrogen Evolution Electrocatalysis" @default.
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• W4286945663 doi "https://doi.org/10.1002/adsu.202200196" @default.
• W4286945663 hasPublicationYear "2022" @default.
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