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• W4288039211 abstract "Abstract A transition‐metal‐free olefinic C−H azidoalkylthiolation protocol was developed through C( sp 3 )−S bond cleavage of vinylsulfonium salts with sodium azide in air under aqueous conditions. An interrupted Pummerer/nucleophilc azidoalkylation cascade was developed for such a process. The practicability of the synthetic protocol was demonstrated by scale‐up preparation of the azidoalkylthiolated tetrasubstituted alkene products and their transformations to diverse triazole and tetrazole derivatives as well as azidoalkylthio‐funtionalized N ‐heterocyclic compounds. The present synthetic methodology features broad substrate scopes and good functional group tolerance under mild conditions. magnified image" @default.
• W4288039211 created "2022-07-27" @default.
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• W4288039211 date "2022-08-09" @default.
• W4288039211 modified "2023-10-18" @default.
• W4288039211 title "Transition‐Metal‐Free Olefinic C−H Azidoalkylthiolation <i>via</i> C(<i>sp</i>³)−S Bond Cleavage of Vinylsulfonium Salts" @default.
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• W4288039211 doi "https://doi.org/10.1002/adsc.202200529" @default.
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