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• W4288696959 abstract "Herein we report the use of indoles, one of the most common nitrogen-containing heterocycles in FDA-approved drugs, as nucleophiles in the Pd-catalyzed aza-Wacker reaction. This N-functionalization of indoles is a Markovnikov selective olefin functionalization of simple alkenes using catalytic Pd(NPhth)2(PhCN)2 and O2 as the terminal oxidant in the presence of catalytic Bu4NBr. Various substituted indoles and alkenes are found to participate; 21 examples are presented with yields ranging from 41 to 97% isolated yield. Additionally, lactams and oxazolidinones are shown to participate under the reaction conditions. Mechanistic investigations suggest that the phthalimide ligand and Bu4NBr additive slow undesired side reactions: indole decomposition and olefin isomerization, respectively." @default.
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• W4288696959 date "2022-07-29" @default.
• W4288696959 modified "2023-09-30" @default.
• W4288696959 title "Palladium-Catalyzed Oxidative Amination of α-Olefins with Indoles" @default.
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• W4288696959 doi "https://doi.org/10.1021/acs.orglett.2c02190" @default.
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