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• W4290998976 endingPage "111675" @default.
• W4290998976 startingPage "111675" @default.
• W4290998976 abstract "Synthesis conditions for preparing [(Ba0.85Ca0.15)0.995Nd0.005](Ti0.9Hf0.1)O3 (Nd-BCTH) nanopowders by hydrothermal method were tailored using orthogonal experiment method with three factors and three levels. X-ray diffraction measurement, field emission scanning electron microscopy, transmission electron microscopy, surface aperture adsorption analyzer, ultraviolet–visible spectra, and fluorescence spectrophotometer were used to characterized the synthesized nanopowders. Well dispersed Nd-BCTH nanopowders with excellent crystallization and luminescence properties are obtained at reaction temperature of 200 °C, 14 mol⋅L−1 alkali concentration, and 24 h reaction time without adding surfactant. The nanopowders present a pure pseudo-cubic perovskite structure with rhombohedral phase approaching the morphotropic phase boundary (MPB) at room temperature, which present nano-sized particles with slight conglomeration. Using 267 nm light exciting, strong photoluminescent emission peaks are excited at 364 nm, 422 nm and 440 nm in the Nd-BCTH nanopowders, which correlate with the transitions of Nd3+ from 4D3/2 → 4I9/2, 2D5/2 → 4I9/2 and 4G11/2 → 4I9/2 via two processes of non-radiative relaxation and fluorescent transition, respectively. The CIE1931 chromaticity calculation of the emission peaks and fluorescent photograph show that the Nd-BCTH nanopowders emit indigo blue fluorescent light." @default.
• W4290998976 created "2022-08-13" @default.
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• W4290998976 date "2022-10-01" @default.
• W4290998976 modified "2023-09-29" @default.
• W4290998976 title "Tailoring synthesis conditions for [(Ba0.85Ca0.15)0.995Nd0.005](Ti0.9Hf0.1)O3 nanopowders by hydrothermal method and their luminescence properties" @default.
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• W4290998976 doi "https://doi.org/10.1016/j.chemphys.2022.111675" @default.
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