Matches in SemOpenAlex for { <https://semopenalex.org/work/W4294762757> ?p ?o ?g. }
Showing items 1 to 83 of
83
with 100 items per page.
- W4294762757 endingPage "32707" @default.
- W4294762757 startingPage "32701" @default.
- W4294762757 abstract "As an antioxidant, N-phenyl-β-naphthylamine (PBNA) inhibits the activity of oxidants, such as NO x , to prevent the degradation of energetic materials. In the presence of NO x , nitrated products can be generated in the process potentially. To characterize nitrated PBNA in a nontargeted analysis of complex samples as such, liquid chromatography tandem quadrupole time-of-flight (LC-QTOF), as an excellent analytic technique, is used due to its high resolution and sensitivity. However, a systematic approach of instrumentation optimization, data interpretation, and quantitative determination of products is needed. Through a step-by-step evaluation of the instrumental parameters used in the Q0, Q1, and Q2 compartments of LC-QTOF, optimal ion yields of precursor ions and high-resolution MS2 fragmentation spectra at low mass defects were obtained in both negative and positive electrospray ionization modes. Through rationalization of the fragmentation pathways and verification using theoretical masses, the mononitro derivative of PBNA was accurately identified as N-(4-nitrophenyl)-naphthalen-2-amine and further confirmed using a reference standard. Using strict criteria provided by the analytical guidelines (e.g., SANTE), limit of quantitation, limit of detection, and calibration were established for the quantitation of PBNA and nitrated PBNA. From optimization to characterization and subsequent quantification of the mononitro-PBNA derivative, for the first time, the applicability of this strategy is demonstrated in the aged energetic binders." @default.
- W4294762757 created "2022-09-06" @default.
- W4294762757 creator A5006480038 @default.
- W4294762757 creator A5031174159 @default.
- W4294762757 creator A5041596191 @default.
- W4294762757 creator A5074286781 @default.
- W4294762757 date "2022-09-06" @default.
- W4294762757 modified "2023-09-30" @default.
- W4294762757 title "Liquid Chromatography Quadrupole Time-of-Flight Mass Spectrometry: A Strategy for Optimization, Characterization, and Quantification of Antioxidant Nitro Derivatives" @default.
- W4294762757 cites W1978734096 @default.
- W4294762757 cites W1992052682 @default.
- W4294762757 cites W2004130289 @default.
- W4294762757 cites W2005796204 @default.
- W4294762757 cites W2006155285 @default.
- W4294762757 cites W2024460618 @default.
- W4294762757 cites W2029165701 @default.
- W4294762757 cites W2063048158 @default.
- W4294762757 cites W2090784036 @default.
- W4294762757 cites W2168407807 @default.
- W4294762757 cites W2325196883 @default.
- W4294762757 cites W2433222289 @default.
- W4294762757 cites W2564497310 @default.
- W4294762757 cites W2746220003 @default.
- W4294762757 cites W2747443481 @default.
- W4294762757 cites W2755493681 @default.
- W4294762757 cites W2964077739 @default.
- W4294762757 cites W2988400645 @default.
- W4294762757 cites W3083271314 @default.
- W4294762757 cites W3094453658 @default.
- W4294762757 cites W3183351987 @default.
- W4294762757 cites W3184815512 @default.
- W4294762757 cites W3209498007 @default.
- W4294762757 cites W4286212722 @default.
- W4294762757 doi "https://doi.org/10.1021/acsomega.2c04376" @default.
- W4294762757 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/36119998" @default.
- W4294762757 hasPublicationYear "2022" @default.
- W4294762757 type Work @default.
- W4294762757 citedByCount "3" @default.
- W4294762757 countsByYear W42947627572022 @default.
- W4294762757 countsByYear W42947627572023 @default.
- W4294762757 crossrefType "journal-article" @default.
- W4294762757 hasAuthorship W4294762757A5006480038 @default.
- W4294762757 hasAuthorship W4294762757A5031174159 @default.
- W4294762757 hasAuthorship W4294762757A5041596191 @default.
- W4294762757 hasAuthorship W4294762757A5074286781 @default.
- W4294762757 hasBestOaLocation W42947627571 @default.
- W4294762757 hasConcept C119128265 @default.
- W4294762757 hasConcept C131779359 @default.
- W4294762757 hasConcept C162356407 @default.
- W4294762757 hasConcept C178790620 @default.
- W4294762757 hasConcept C185592680 @default.
- W4294762757 hasConcept C43617362 @default.
- W4294762757 hasConceptScore W4294762757C119128265 @default.
- W4294762757 hasConceptScore W4294762757C131779359 @default.
- W4294762757 hasConceptScore W4294762757C162356407 @default.
- W4294762757 hasConceptScore W4294762757C178790620 @default.
- W4294762757 hasConceptScore W4294762757C185592680 @default.
- W4294762757 hasConceptScore W4294762757C43617362 @default.
- W4294762757 hasFunder F4320338304 @default.
- W4294762757 hasIssue "36" @default.
- W4294762757 hasLocation W42947627571 @default.
- W4294762757 hasLocation W42947627572 @default.
- W4294762757 hasLocation W42947627573 @default.
- W4294762757 hasLocation W42947627574 @default.
- W4294762757 hasLocation W42947627575 @default.
- W4294762757 hasOpenAccess W4294762757 @default.
- W4294762757 hasPrimaryLocation W42947627571 @default.
- W4294762757 hasRelatedWork W1845624145 @default.
- W4294762757 hasRelatedWork W1976257423 @default.
- W4294762757 hasRelatedWork W1980714464 @default.
- W4294762757 hasRelatedWork W1987755785 @default.
- W4294762757 hasRelatedWork W1988317878 @default.
- W4294762757 hasRelatedWork W1994651367 @default.
- W4294762757 hasRelatedWork W2033364217 @default.
- W4294762757 hasRelatedWork W2075761790 @default.
- W4294762757 hasRelatedWork W2130473357 @default.
- W4294762757 hasRelatedWork W377763774 @default.
- W4294762757 hasVolume "7" @default.
- W4294762757 isParatext "false" @default.
- W4294762757 isRetracted "false" @default.
- W4294762757 workType "article" @default.