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- W4294904760 endingPage "109954" @default.
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- W4294904760 abstract "Both the barium strontium titanate as well as its respective selenium doped sample were synthesized through a slow injection sol–gel method which is calcined at 800 0C. The microstructural and morphological effects have been explored using XRD, BET, FE-SEM, TEM, EDS, XPS and FT-IR. The existence of Se in Se-doped BST was initially confirmed by EDS which was later firmly established by the XPS. Se was found in the BST base material as Se6+3d5/2 with a binding energy of 61.0 eV. The wave numbers of Ba-O, Ti-O, Sr-O bonds of Se-doped BST shifted from the respective values for the BST nanopowders. The addition of Se into BaxSr1-xTiO3 led to the reduction of an average crystal size from 23.97 nm to 20.68 nm and lattice parameter from 3.97 Å to 3.93 Å On the other hand, the particle size of BST has been lowered from 40.125 nm to 16.806 nm after doping. The specific surface area has also been lowered from 557.9 m2/g to 539.5 m2/g leading to the reduction of pore size and pore volume along with elevation of aggregates of particles from 6.42x10-4 to 1.1x10-3. The morphology of Se-doped BST was found with increased surface roughness as compared to the BST. Hence, the Se-doped Ba0.6Sr0.4TiO3 has shown varied structural and morphological properties from the Ba0.6Sr0.4TiO3." @default.
- W4294904760 created "2022-09-07" @default.
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- W4294904760 date "2022-11-01" @default.
- W4294904760 modified "2023-09-25" @default.
- W4294904760 title "The microstructural and morphological effects of doping barium strontium titanate nanocrystalline with selenium" @default.
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- W4294904760 doi "https://doi.org/10.1016/j.inoche.2022.109954" @default.
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