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- W4296551299 abstract "The spiroketal moiety is an important substructure within many biological natural products. One method to access them is via the oxidative cyclisation of a pendant hydroxyl group on to a pre-formed pyran. However access to such precursors has hitherto been challenging and requires multistep syntheses frequently with considerable protecting group manipulation. Herein we report a novel and high yielding method for the preparation of hydroxydi- and hydroxytetra-hydropyrans, as spiroketal precursors, utilizing a novel double-Prins cyclisation approach." @default.
- W4296551299 created "2022-09-21" @default.
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- W4296551299 date "2022-10-25" @default.
- W4296551299 modified "2023-09-24" @default.
- W4296551299 title "Double Prins Cyclisation Enabled Rapid Access to α,ω‐Hydroxytetrahydropyrans" @default.
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- W4296551299 doi "https://doi.org/10.1002/ejoc.202200810" @default.
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