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• W4296848696 endingPage "121924" @default.
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• W4296848696 abstract "• Glasses with Al 2 O 3 produced higher sulfate retention and solubility. • Eskolaite formation occurred in glasses containing both Al 2 O 3 and sulfur. • Chromium source did not affect observed overall behavior regarding sulfur. • Salt phase formed was Na 2 (S,Cr)O 4 with a S>Cr. The presence of sulfur-containing molten salt phases during vitrification is a particular problem which can be detrimental to the melter. Borosilicate compositions were designed to explore both the effects of a fixed amount of Cr, as Cr 2 O 3 or Na 2 CrO 4 , and the impact of Al 2 O 3 , on sulfur solubility as determined by progressively adding elemental S. The NABS series (with Al 2 O 3 ) has a higher SO 3 solubility of ∼3.5 mol% while the NBS series (without Al 2 O 3 ) has a SO 3 solubility of ∼2 mol%. Crystalline Cr 2 O 3 formed in the NABS series upon the addition of S but is not present in the NBS series. At the highest S addition, a separate salt phase always forms, and was identified as Na 2 (S,Cr)O 4 via electron dispersive spectroscopy, ultraviolet-visible spectroscopy, x-ray diffraction, and thermal analysis. Magic angle spinning nuclear magnetic resonance identified no change in the B coordination in either series as S is added, suggesting that the Na is scavenged from other locations, such as the Si sites, to charge compensate sulfate, whether in the glass or in the salt. The Cr precursor identity did not affect the observed overall behavior regarding sulfur, but did impact Cr redox as identified with Raman spectroscopy." @default.
• W4296848696 created "2022-09-24" @default.
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• W4296848696 date "2022-12-01" @default.
• W4296848696 modified "2023-10-14" @default.
• W4296848696 title "The S solubility of Cr and Al containing simulated low-activity waste glass" @default.
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• W4296848696 doi "https://doi.org/10.1016/j.jnoncrysol.2022.121924" @default.
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